Solid superacid catalyzed fatty acid methyl esters production from acid oil

Author

Yan Li, Xiao-Dong Zhang, Li Sun, Min Xu, Wen-Guang Zhou and Xiao-Hui Liang

Applied Energy, 2010, vol. 87, issue 7, pages 2369-2373

Abstract: A solid superacid catalyst was evaluated for the production of fatty acid methyl esters (FAMEs) from acid oil containing about 60 wt.% free fatty acids. It was demonstrated that /ZrO2-TiO2/La3+ was an effective catalyst for simultaneous transesterification and esterification. The optimization of reaction parameters was performed, showing that maximum yield of above 90% could be obtained under the conditions that molar ratio of alcohol/oil was 15:1, catalyst amount was 5 wt.%, temperature was 200 °C and duration was 2 h. The catalyst was finally recycled and utilized for five times repeatedly with little loss in activity. The final products purified by molecular distillation were detected by GC-MS. The content of FAMEs reached 96.24%.

Keywords: Solid; superacid; catalyst; Fatty; acid; methyl; esters; Acid; oil (search for similar items in EconPapers)
Date: 2010
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